中文摘要：

以富勒烯乙二胺硝酸盐和二硝酰胺铵（ADN）为原料,通过离子交换反应制备了富勒烯乙二胺二硝酰胺盐,采用紫外-可见光谱（UV-Vis）、傅里叶变换红外光谱（FT-IR）、元素分析和X射线光电子能谱（XPS）等对其结构进行了表征.结果表明,富勒烯乙二胺二硝酰胺盐的分子式为H12C60（HNCH2CH2NH2·HN（NO2）2）12.用差热分析（DTA）、差示扫描量热法（DSC）和热重-微分热重分析（TG-DTG）研究其热分解特性.DSC曲线表明富勒烯乙二胺二硝酰胺盐于150℃开始分解,热分解峰温为203℃,分解焓为1037.7 J·g^-1.TG曲线表明,100～800℃范围内,总失重率49.68％,主要是N（NO2）2-分解和部分支链分解.

英文摘要：

Fullerene ethylenediamine dinitramide was synthesized via ion exchange reaction of fullerene ethylenediamine nitrate and ammonium dinitramide （ADN）. The structure offullerene ethylenediaminedinitramide was characterized by UV-Vis, FT-IR, elemental analysis and XPS. Its thermal decomposition characteristics were investigated by thermogravimetric-differential thermo- gravimetry （TG-DTG）, differential scanning calorimetry （DSC） and differential thermal analysis （DTA）. Results show that the molecular formula of fullerene ethylenediamine dinitramide is H12C60（HNCH2CH2NH2 · HN（NO2）2）12. DSC curve shows that fullerene ethylenediamine dinitramide starts to decompose at 150 ℃ with thermal decomposition peak temperature 203 ℃ and decomposition enthalpy 1037.7 J · g^-1. TG study indicats the total mass loss in the temperature range 100-800 ℃ is 49.68% with intense decomposing of N（ NO2）-2 and part of the branched chain decomposing.