在这篇论文,传统的 milling 和分泌物,帮助血浆的 milling 被采用综合在由 milling 的纳米规模的铝氮化物(AlN ) 粉末铝和锂氢氧化物一水化物的混合。AlN 粉末能在一小时 milling 时间在传统的 milling 和帮助血浆的 milling 被产生。微分热分析曲线证明帮助血浆的 milling 对待的粉末的反应温度比传统的 milling 的低。这些结果显示帮助血浆的 milling 在 AlN 的合成有更高的效率,得到更小的雏晶尺寸并且激活粉末。而且,一个光排放系列被采用在血浆表明活跃种类。在二工厂的过程的 AlN 的不同形成过程,和在 milling 过程的血浆的提升效果被讨论。
In this paper,traditional milling and discharge plasma-assisted milling are employed to synthesize aluminum nitride(AlN) powder at nanometer scale by milling the mixture of aluminum and lithium hydroxide monohydrate.AlN powders can be generated in traditional milling and plasma-assisted milling in an hour milling time.Differential thermal analysis curves show that the reaction temperature of the powders treated by plasma-assisted milling is lower than that of traditional milling.These results indicate that plasma-assisted milling has higher efficiency in the synthesis of AlN,getting smaller crystallite size and activating powder.Moreover,an optical emission spectrum is employed to demonstrate the active species in plasma.The different formation process of AlN in the two-milling process,and the promotion effects of plasma in the milling process are discussed.