采用声化学法、放电等离子烧结技术(SPS)和热变形工艺制备致密各向同性和各向异性Nd2Fe14B/α-Fe复合磁体,研究了软磁相包覆对磁体的结构和性能的影响.结果表明,软磁相α—Fe对各向同性Nd2Fe14B/α—Fe复合磁体的影响主要表现为增强两相间的交换耦合作用,从而提高剩磁.当α—Fe体积分数的数值适当(不超过2%)时,各向异性 Nd2Fe14B/α—Fe磁体形成较好的c轴晶体织构,具有较高的磁性能.α—Fe体积分数为1%的磁体性能最高:Br=1.367T,Hci=712 kA/m,(BH)m=327kJ/m^3.
Full dense isotropic and anisotropic Nd2Fe14B/α-Fe nanocomposite magnets were prepared via sonochemistry method, spark plasma sintering (SPS) and hot deformation method. The effects of α-Fe volume fraction on the structure and magnetic properties of the magnets were investigated. For the isotropic magnets, the exchanging coupling and remanence increase as the α-Fe content increases. For the anisotropic magnets, only the magnets with no more than 2% α-Fe exhibit strong c-axis crystal texture of Nd2Fe14B phase, and the better magnetic properties are Br=1.367 T, Hci=712 kA/m, (BH)m= 327 kJ/m^3.