静电纺丝法是一种制备超细纳米纤维的简单有效的方法,已用于多种材料的制备.近几年来,有彬无机复合纳米纤维由于其优异的性能已被广泛地应用于化学(生物)防护、药物传输、能量产生及存储、高性能选择过滤、气体传感器等方面.
Poly( vinyl pyrrolidone) (PVP)/Fe3O4 composite nanofibers were successfully prepared by using electrospinning technique. The composite nanofibers were characterized by means of TEM ( transmission electron microscopy), XRD( X-ray diffraction) and TGA( thermogravimetric analysis). Transmission electron microscope images of the PVP/Fe3O4 nanofibers show that the Fe3O4 nanoparticles with a diameter about 10. 5 nm were dispersed in PVP fiber matrices. The XRD results show that the particles in PVP fibers were indeed Fe3O4 nanoparticles. And the TGA of PVP/Fe3O4 nanofibers show that the content of Fe3O4 nanoparticles in the composite was about 36.8% (mass fraction). The PVP/Fe3O4 nanofibers were found to be superparamagnetic. The hysteresis loop at room temperature showed a high saturated magnetization (Ms = 15.1 emu/g) and a low coercive force (μc = 0).