为寻求简单快速合成金属催化剂配体化合物西佛碱的方法,利用微波驱动的有机反应具有快速高效的优点,于无溶剂、616W微波功率驱动下,20s~4 min快速高效合成了6种水杨醛亚胺类化合物.化合物的化学结构经IR,NMR和元素分析测试加以证实.
A simple and rapid method for the preparation of Schiff-base compounds as the ligands of catalysts,has been designed a microwave-assisted condensation of salicylaldehyde and amines without solvent and catalyst were efficiently performed to form a series of salicylaldimines in high yields, which were confirmed by IR, NMR and elemental analyses.