采用双酚A型wSR-615和缩水甘油胺型AG-80环氧树脂为基体,以Fe-Si磁性颗粒为填料,通过热压成型方法制备了高含量磁性Fe-si颗粒/环氧树脂复合材料。研究了环氧树脂基体的玻璃化温度和冲击强度及Fe-Si磁性颗粒含量对Fe-Si/环氧树脂复合材料的冲击强度和磁化强度的影响及温度敏感性。研究结果表明:随着磁性颗粒含量的增加,Fe-Si/环氧树脂复合材料的冲击强度和磁性能增加。当磁性颗粒体积分数由54vol%增加到66v01%时,Fe-si/环氧树脂的冲击强度和饱和磁化强度分别由4.03kJ/m2和162.07emu/g增加到7.16kJ/m2和175.04emu/g。Fe-si/环氧复合材料在-60℃~140℃范围内的温度敏感性低,符合实际应用对复合材料稳定性的要求。
The magnetic composites were prepared by mixing bisphenols A WSR-615 and glycidyl amine AG-80 epoxy resins and a high content of Fe - Si magnetic particles using hot- pressing process. The glass transition temperature and impact property of the epoxy resins and the impact strength and magnetization of the composites were investigated as a function of Fe - Si content and temperature. It is shown that the impact strength and the magnetization of Fe - Si/epoxy composites increase with increasing the Fe - Si content and are enhanced from 4.03 kJ/m2 and 162.07 emu/g to 7.16 kJ/m2 and 175.04 emu/g at 54 vol% to 66 vol% Fe - Si particles. The impact strength and magnetization of the composites are very lightly sensitive to the temperature change from --60 ℃ to 140 ℃, which is desired for practical applications requiring that the mechanical and magnetic properties are stable as the temperature changes.