摘要在高温高压(5.0GPa、1500℃)的条件下,以Ni7。Mn25C05合金为烧结助剂,采用粉末混合法制备了金刚石复合片(PDC),并采用SEM及Micro-Ramanspectroscopy对金刚石烧结体进行了形貌及物相测试。结果表明,由于烧结腔体存在压力、温度梯度,金刚石在经历高温高压烧结后,具有多种烧结形态及物相结构,表现为晶形完整的金刚石微晶、纳米石墨相和无定形碳。
Under the high temperature and high pressure (5.0 GPa, 1500 ~C) conditions, PDC was prepared by mix-powder method using Ni70 Mn25 Co5 alloy as sintering aids. SEM and Micro-Raman spectroscopy were used to investigate the morphology and structure of diamonds sintered body, and the results show that the diamonds, after sintering at high pressure and high temperature, have a variety of carbon phase structure because of the existence of sintering pressure and temperature gradient, performing for the perfect micro-crystal of diamonds, nano-graphite and amorDhous carbon.