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快速生长KDP晶体表面的光学显微实时观察
  • 期刊名称:人工晶体学报
  • 时间:0
  • 页码:598-602
  • 分类:O782.1[理学—晶体学]
  • 作者机构:[1]青岛大学物理科学学院,青岛266071
  • 相关基金:国家自然科学基金(No.10774081 No.10979029); 国家光电子晶体材料工程技术研究中心开放基金(2007K08); 山东省自然科学基金(Y2007F16)
  • 相关项目:同步辐射法研究BIBO与KDP晶体特征生长机制与缺陷
中文摘要:

设计了一套溶液降温法晶体生长显微实时观察装置,对快速生长KDP晶体{101}和{100}表面形貌的演化过程进行了实时观测分析。测量了晶体表面生长层切向生长速度随溶液过饱和度的变化曲线,并利用台阶生长动力学方程计算了相关动力学参数。进行了Fe3+掺杂实验,结果表明Fe3+的存在会影响到不同晶面上生长层的动力学系数,从而改变KDP晶体表面生长层的切向生长速度。

英文摘要:

A set of device for in-situ observing crystal growth by temperature lowering method in solution was designed.The evolution of the {100} and {101} surface morphology of the rapid growing KDP crystal was in-situ observed and analyzed.The curves of growth layers tangential velocity on the solution supersaturation were measured.Kinetic parameters were computed by steps growth kinetics formula.The Fe3+ doping experiments were carried out.It was found that Fe3+ could change the kinetics coefficients of growth layers on different crystal faces,and consequently affects the tangential growth velocity of the growth layers.

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