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中文摘要：
利用二硫化碳与水不混溶的特点,设计了油相为溶有单质硫的二硫化碳溶液、水相为金属盐水溶液的两相体系,在100℃溶剂热条件下发生反应,制备出具有不同微/纳结构的系列金属硫化物,如CdS、PbS和CuS枝晶、ZnS微米球和Ag2S花生状纳米球结构等,证实了该合成方法具有通用性。通过X射线衍射（XRD）、透射电子显微镜（TEM）和场发射扫描电子显微镜（FE-SEM）等手段对产物进行成分与结构的表征,提出了油-水界面反应制备微/纳结构金属硫化物的可能机理,并用荧光分光光度计（PL）对产物的光学性质进行了研究。
英文摘要：
A series of micro/nano metal sulfides such as CdS,PbS and CuS dendrites,ZnS microspheres,Ag2S peanut-like nanospheres have been synthesized by the solvothermal reactions between metal salt aqueous solution and CS2 solvent dissolved with sulfur at 100 ℃.The products were characterized by X-ray diffraction（XRD）,transmission electron microscopy（TEM） and field-emission scanning electron microscopy（FE-SEM） and the optical properties were investigated through photoluminescence（PL） spectroscopy.The possible mechanism for preparing micro/nano metal sulfides at the oil-water interface is suggested.
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