以三方相t-Se纳米管为模板,N2H4·H2O为还原剂的碱性溶液中室温合成硒化镍纳米管。产物分别用扫描电子显微镜(SEM)、X射线衍射仪(XRD)、X射线光电子能谱(XPS)等表征手段进行表征。利用循环伏安法研究了硒化镍纳米管在不同介质中的电化学行为,探讨了电解质对硒化镍纳米管电化学性质的影响。
The NiSe2 nanotubes were synthesized at room temperature using t-Se nanotubes as a template and N2H4 ·H2O as a reductant in alkalescent solution. The structure of the NiSe2 nanotubes was characterized using scanning electron microscope (SEM), X-ray powder diffraction (XRD) and X-ray photoelectronic spectroscopy (XPS). The formation mechanism of NiSe2 nanotubes was investigated. The electrochemical property of NiSe2 nanotubes was researched by cyclic voltammetry method in different medium solution.