位置:成果数据库 > 期刊 > 期刊详情页
氦离子辐照对镍基合金硬度的影响
  • ISSN号:0253-3219
  • 期刊名称:《核技术》
  • 时间:0
  • 分类:TL34[核科学技术—核技术及应用]
  • 作者机构:[1]中国科学院上海应用物理研究所嘉定园区,上海201800, [2]中国科学院大学,北京100049, [3]中国科学院核辐射与核能技术重点实验室,上海201800, [4]上海科技大学,上海200031
  • 相关基金:国家自然科学基金培育项目(No.91126012)、上海市自然科学基金(No.14ZR1448300)资助
中文摘要:

在室温下对镍基合金进行了氦离子辐照,利用纳米压痕仪测试了微观硬度,利用慢正电子多普勒展宽谱(Doppler Broadening Spectrum, DBS)和透射电子显微镜(Transmission Electron Microscope, TEM)分析了微观缺陷,利用离子束分析弹性反冲探测(ElasticRecoilDetection,ERD)技术测量了氦的浓度深度分布。结果显示合金样品的硬度随剂量而增大,退火后合金样品硬度增量有所减小,并观测到氦泡生成。合金硬化的主要原因是由于氦离子辐照产生了1-7nm的缺陷团簇,而退火后不稳定缺陷的回复及氦.空位复合体数量的减少造成了硬化强度减弱。

英文摘要:

Background: Hastelloy-N alloy is selected as the structural material for molten salt reactor (MSR), however, it is well-known that helium atoms play an important role in nickel-based materials after severe neutron irradiation, since they can drastically alter mechanical properties, potentially embrittle materials even at low concentration. Purpose: This study aims to understand the hardening of Hastelloy-N alloy material caused by helium irradiation. Methods: Samples were irradiated by helium ions of various energies and intensities at room temperature. After annealed at temperature of 773 K, 873 K and 973 K separately, and some typical samples annealed at 873 K were chosen as objects of investigation. Nano-indentation technique was used to obtain the hardness; elastic recoil detection (ERD) was used to detect the helium concentration; and positron annihilation spectroscopy (PAS) was used to investigate S parameter. The microstructure was characterized by transmission electron microscopy (TEM). Results: The hardness of the Hastelloy-N alloys irradiated by He+ increased with the dose whilst the S parameter first increased with irradiation dose, but decresed after reach certain incident depth. After annealing, both the hardness and the S parameters decreased. The TEM image showed lots of radiation-induced defects after irradiation. The small defects were annihilated and 1-nm small helium bubble was observed after annealing. Conclusion: The large radiation-induced defects were believed to be the causes of the hardening. While the recovery of hardening after 873 K annealing was ascribed to the annihilation of the small defects, the desorption of helium and the decreasing number of HenVm.

同期刊论文项目
同项目期刊论文
期刊信息
  • 《核技术》
  • 北大核心期刊(2011版)
  • 主管单位:中国科学院
  • 主办单位:中国科学院上海应用物理研究所 中国核学会
  • 主编:朱德彰
  • 地址:上海800-204信箱
  • 邮编:201800
  • 邮箱:LHB@sinap.ac.cn
  • 电话:
  • 国际标准刊号:ISSN:0253-3219
  • 国内统一刊号:ISSN:31-1342/TL
  • 邮发代号:4-243
  • 获奖情况:
  • 2000年中科院优秀期刊奖,中国中文核心期刊,中国期刊方阵“双效”期刊
  • 国内外数据库收录:
  • 美国化学文摘(网络版),荷兰文摘与引文数据库,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),英国英国皇家化学学会文摘,中国北大核心期刊(2000版)
  • 被引量:7912