采用索氏提取法对中草药川楝子进行粗提,通过乙醚蒸发仪进行无水浸提,提取出的高纯度挥发油经气质联用仪分析,检测出川楝子挥发油中的5种主要成分:2,3-Dimethylpentance;3,3,4-trimethylhexa;3-methyl-6-methylene;2,4,4-trimethylhexa;1,3-dimethylcycl。通过原子吸收光谱仪对川楝子中微量元素的成分与数量进行测定,检测出川楝子中6种微量元素的含量排序为K〉Mg〉Na〉Fe〉Ca〉Zn。研究结果为川楝子药物的开发与应用提供了科学依据。
Chinese herbal medicine fructus toosendan is extracted by Soxhlet extraction method. After anhydrous extraction by ether evaporation instrument, the pure essential oil is finally ob- tained. Using gas chromatography - mass spectrometry analysis, five main components of volatile oil in fructus toosendan are identified: 2, 3- Dimethylpentance, 3, 3, 4- trimethylhexa, 3- methyl - 6 - methylene, 2, 4, 4 - trimethylhexa and 1,3 - dimethylcycl. In addition, the com- position and quantity of trace elements in the samples were determined by atomic absorption spectrometry. Six kinds of trace elements were detected, the content of which was K 〉 Mg 〉 Na 〉 Fe 〉 Ca 〉 Zn. The results of this study provide scientific basis for the development and application of fructus toosendan.