采用一种新工艺处理的BPPM反应液。讨论了新工艺流程,在新工艺条件下BPPM的收率达到69.5%。与文献报道的原工艺相比,反应收率提高7.7%,产品纯度大于99.9%,且工艺操作更简单。
A new process was adopted to treat BPPM reaction solution.The new precess was discussed and the title compound was obtained to be 69.5% under the new process conditions.The yield of BPPM is 7.7% higher than that of classical literature.The purity of product is over 99.9%.The process operations are more convenient.