通过铝热法制备了Cu含量为2%,4%,6%(质量分数,下同)的Fe3Al-10%Ni块体纳米晶材料,用光学显微镜(OM),电子探针(EPMA),X-射线衍射仪(XRD)和透射电镜(TEM)表征了材料的微观结构,并测定了材料的维氏硬度和室温压缩性能。结果表明:Cu含量低(2%)时,合金保持无序bcc结构,晶粒尺寸显著下降;高Cu含量(4%和6%)使合金发生B2型有序化转变。添加Cu元素提高了材料的硬度,但不利于材料塑性的提高。添加2%和6%的Cu元素使材料的屈服强度明显增加,而添加4%的Cu元素使材料的强度明显下降。
Effects of Cu additions on microstructure and mechanical properties of Fe3Al-10%Ni bulk nanocrystalline prepared by aluminothermic reaction were studied.The microstructure was studied by OM,EPMA,XRD and TEM,and the hardness and compressive strength were measured.The results reveal that the low Cu content(2%) maintained the bcc crystal structure and resulted in a sharp decrease of the average grain size.However,high Cu contents(4% and 6%) caused the structure ordering to B2.The hardness increased after adding Cu.A high Cu content was not benefit to the plasticity.The yield strength increased slightly at 2% and 6% Cu,but decreased a lot at 4% Cu.