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Synthesis of a 1,2,7,8-tetraoxa-spiro[5.5]undecane
  • ISSN号：1001-604X
  • 期刊名称：中国化学(英文版)
  • 时间：0
  • 页码：1304-1308
  • 语言：中文
  • 分类：R962[医药卫生—药理学;医药卫生—药学]
  • 作者机构：[1]State Key Laboratory of Bio-Organic and Natural Products Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China
  • 相关基金：Project supported by the National Natural Science Foundation 0f China （Nos. 20025207, 20272071, 20372075, 20321202, 20672129, and 20621062）, and the Chinese Academy of Sciences （Nos. NKGCX2-SW-209 and KJCX2.YW.H08）.
  • 相关项目：若干具抗菌、抗肿瘤等活性的天然产物及其类似物的不对称全合成研究
作者： Wu, Yi-Kang|Li, Yun|Zhang, Qi|
关键词： 抗疟药, 过氧化物, 药物合成, 药物化学, peroxide, antimalarial, artemisinin, hydrogen peroxide, spiro compound
中文摘要：

新 spiro 的合成器官的过氧化物被描述。peroxy 契约作为 peroxy 连接的来源用氢过氧化物经由催化酸的 ketal 交换反应被合并到底层框架。hydroperoxyl 组然后经由导致的 Hg (II ) 在 OH 结束被结合 C-C 的 electrophilic 增加加倍契约，在每二枚六成员的戒指与一张 peroxy 契约给新奇 sprio 结构。在方面链的酉旨功能也使进行进一步结构的修正可能。

英文摘要：

Synthesis of a new spiro organic peroxide is described. The peroxy bonds were incorporated into the substrate framework via an acid-catalyzed ketal exchange reaction using hydrogen peroxide as the source of peroxy linkage. The hydroperoxyl groups were then bonded at the OH ends via Hg（II）-induced electrophilic additions to the C-C double bonds, giving a novel sprio structure with one peroxy bond in each of the two six-membered rings. The ester functionalities in the side chains also make it possible to conduct further structural modifications.

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期刊信息
  • 《中国化学：英文版》
  • 主管单位:
  • 主办单位:中国化学会
  • 主编：
  • 地址：上海市枫林路354号中科院上海有机化学研究所
  • 邮编：200032
  • 邮箱：
  • 电话：021-54925243
  • 国际标准刊号：ISSN：1001-604X
  • 国内统一刊号：ISSN：31-1547/O6
  • 邮发代号:4-646
  • 获奖情况:
  • 中国期刊方阵“双高”期刊
  • 国内外数据库收录:
  • 美国化学文摘（网络版）,荷兰文摘与引文数据库,美国科学引文索引（扩展库）,日本日本科学技术振兴机构数据库,英国英国皇家化学学会文摘
  • 被引量:175