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牙科热压铸造工艺对牙科低熔云母玻璃陶瓷显微结构的影响
  • 期刊名称:实用口腔医学,2008,24(6):806-810.
  • 时间:0
  • 分类:R783.1[医药卫生—口腔医学;医药卫生—临床医学]
  • 作者机构:[1]第四军医大学口腔医学院修复科,西安 710032, [2]西安交通大学材料强度国家重点实验室
  • 相关基金:国家自然科学基金(50672127)
  • 相关项目:低熔点高韧性可延性切削牙科云母微晶玻璃陶瓷的应用基础研究
中文摘要:

目的分析不同晶化温度和晶化时问对一种氟金云母玻璃陶瓷加工性能的影响,探讨其延性切削行为的机制。方法使用SiO2-B2O3-R2O—Al2O3-ZnO—MgO—F(R为碱金属)玻璃陶瓷粉制备晶化温度和晶化时间分别为650℃(60min)、680℃(60min)、710℃(60min)、740℃(60min)、680℃(30min)、680℃(120min)、680℃(240min)的试件,分为A、B、C、D、E、F、G组,每组6个;长石质可切削陶瓷试件作为对照组。测定8组试件钻孔30s后的钻孔深度,并进行车床切削实验定性分析。扫描电镜和X射线衍射分析观察试件的微观结构。结果A组钻孔深度最大,为(7.1±0.8)mm;D组最小,为(0、5±0.1)mm。除D组外,其余组钻孔深度均大于对照组[(0.8±0.1)mm],差异均有统计学意义(P〈0.05)。A组试件可在普通车床高速车削条件下形成连续带状切屑,其晶体相含量约为40%。结论这种云母玻璃陶瓷具有良好的可加工性,其机制可能与云母晶体的互锁结构和玻璃相黏滞流动作用相关。

英文摘要:

Objective To investigate the machinability of a novel dental mica glass-ceramic and analyze the effect of heat-treatment on its ductile machinable behavior. Methods The drilling and turning experiment were used to measure the machinabilities of the control group (feldspar ceramic: Vita Mark 11 ) and 7 experiment groups treated with different crystallization techniques. The microstructures were analyzed using scanning electron microscopy ( SEM ) and X-ray diffraction ( XRD ). Results The average drilling depths in 30 s of the experimental groups ranged from ( 0. 5 ±0. 1 ) mm to ( 7. 1 ± 0. 8 ) mm. There were significant differences between the control [ ( 0. 8 ±0. 1 ) mm ] and the experimental groups ( P 〈 0. 05 ) except the group crystallized at 740 ℃ for 60 min. When crystallized at 650 ℃(60 min) ,continuous band chips could formed in machining at a high velocity and cut depth. The crystal portion of this group is only about 40%. Conclusions This material has a satisfactory machinability. The mechanism could be attributed to a combination of the interlocked structure of mica crystals and the low viscosity of glassy phase.

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