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炭/炭复合材料表面预炭层的制备及其性能研究
  • 期刊名称:无机材料学报, 2009, 24 (1): 125-128. (SCI:00026253480002
  • 时间:0
  • 分类:TB332[一般工业技术—材料科学与工程]
  • 作者机构:[1]西北工业大学炭/炭复合材料工程技术研究中心,西安710072
  • 相关基金:基金项目:国家自然科学基金(90716024);“111”引智工程项目(08040);国家“973”资助项目(2006CB600908)
  • 相关项目:非烧蚀碳/碳—碳泡沫组合结构材料一体化设计及制备技术研究
中文摘要:

为在炭/炭复合材料表面制备C/SiC浓度梯度高温抗氧化涂层,预先用料浆涂刷-高温处理工艺在其表面制备了预炭层.借助XRD、Ram an和SEM等测试手段对所制备预炭层的组织结构和微观形貌进行了表征,讨论了不同的原料配比和炭化温度对预炭层结构的影响,并对预炭层与基体的结合性能进行了测定.研究结果表明:制备的预炭层结构致密,与基体具有较好的结合性能,其结合强度可达10.95MPa.不同的原料配比和炭化温度影响了炭层序态结构的形成,最终形成了不同结构的预炭层.

英文摘要:

Pre-coated carbon layers on the surface of carbon/carbon composites were prepared firstly by slurry and high-temperature treatment for preparing the anti-oxidation coating with SiC concentration gradient. The micrographs and microstructures of the pre-coated carbon layer were characterized by SEM, Raman and XRD. The effects of different graphite content and carbonization temperature on the microstructure of precoated carbon layer were investigated. The bonding strength between the carbon layer and the C/C composites was also measured. The results show that the as-prepared carbon layer is dense and the bend strength reaches 10.5MPa. The structures of the pre-coated carbon layer are influenced by the graphite content and carbonization temperature, and the pre-coated carbon layers with different structures are obtained.

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