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两类钒基合金的辐照硬化研究
  • ISSN号:0253-3219
  • 期刊名称:《核技术》
  • 时间:0
  • 分类:TL99[核科学技术—核技术及应用]
  • 作者机构:[1]中国科学院近代物理研究所,兰州730000, [2]中国科学院大学,北京100049, [3]北京有色金属研究总院国家有色金属及电子材料分析测试中心,北京100088
  • 相关基金:国家自然科学基金委大科学装置联合基金(No.U1532262)、国家磁约束核聚变能研究发展计划专项(No.2011GBl08003)资助
中文摘要:

钒合金(V-Cr-Ti系列)是重要的聚变堆结构候选材料,但是相比于铁素体/马氏体钢等其他候选材料,有关钒合金(V-Cr-Ti)的辐照损伤研究较为缺乏。利用载能离子束模拟聚变堆中子辐照条件,对V-4Cr-4Ti和V-5Cr-5Ti两种样品进行了载能He离子和重离子辐照实验。实验采用离子束梯度减能方法在样品中产生辐照损伤的坪区,利用纳米压痕技术测试材料的辐照硬化效应。结果表明,样品纳米硬度的深度递减现象可以用Nix-Gao模型很好描述,高能重离子辐照的样品中软基体效应可以有效避免;在He离子辐照情形,He浓度(以原子百万分率计(Atomic parts per million,APPM))/位移损伤(以每原子平均离位数计(Displacement per atom,DPAl)大于4200/0.2时,两种钒合金样品出现硬化饱和现象;相近位移损伤水平下,He与空位的结合导致缺陷集团的加速长大,致使材料的辐照硬化远大于重离子辐照情形。

英文摘要:

Background: Vanadium alloy (V-Cr-Ti) is an important fusion reactor candidate material due to its low activation characteristics, desirable high-temperature strength and good resistance to radiation damage. However, studies at lower temperature have shown a substantially reduced radiation resistance, manifested in a loss of ductility and enhanced hardening. Purpose: This work aims to investigate the irradiation hardening behavior of vanadium alloys under He-ion implantation and displacement damage, and provide an experimental evidence for optimizing the radiation resistance of vanadium alloys. Methods: In this study, irradiation of V-4Cr-4Ti alloy and V-5Cr-5Ti alloy samples were carried out with He-ions and swift-heavy-ions. A thick layer with a uniform damage distribution in samples was produced by varying energy of He ions, or by using an energy degrade wheel for swift-heavy-ion irradiation. The nanoindentation technique was used to measure the irradiation hardening. Cross-sectional transmission electron microscopy (TEM) sample fabricated from the irradiated samples were investigated with TEM. Results: The results show that the hardening saturation occurs when the dose of He-ion implantation is more than 4 200 (Atomic parts per million, APPM)/0.2 (Displacement per atom, DPA). The irradiation hardening by He-ions is far larger than that by the swift-heavy-ions at the same displacement damage level. Conclusion: The phenomenon of the enhanced hardening by He-ions can be attributed to the accelerated formation of defect clusters due to the combination of He-atoms and vacancies.

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期刊信息
  • 《核技术》
  • 北大核心期刊(2011版)
  • 主管单位:中国科学院
  • 主办单位:中国科学院上海应用物理研究所 中国核学会
  • 主编:朱德彰
  • 地址:上海800-204信箱
  • 邮编:201800
  • 邮箱:LHB@sinap.ac.cn
  • 电话:
  • 国际标准刊号:ISSN:0253-3219
  • 国内统一刊号:ISSN:31-1342/TL
  • 邮发代号:4-243
  • 获奖情况:
  • 2000年中科院优秀期刊奖,中国中文核心期刊,中国期刊方阵“双效”期刊
  • 国内外数据库收录:
  • 美国化学文摘(网络版),荷兰文摘与引文数据库,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),英国英国皇家化学学会文摘,中国北大核心期刊(2000版)
  • 被引量:7912