中文摘要：

在四氢呋喃／水混合相溶剂中，以锌粉参与的经典烯丙基化反应合成了标题化合物，利用核磁（1HNMR）、红外光谱和质谱（LRMS）表征了其结构，利用气相色谱仪测试了其纯度，并讨论了甲代烯丙基溴与锌粉的物质的量比、反应时间及温度等影响因素，确定了该反应的最佳条件；同时，在甲苯／水混合相溶剂中和少量醋酸作用下，以甲代烯丙基氯为起始原料合成了标题化合物，原料易得，操作方便，具有应用于工业化生产的潜力。

英文摘要：

The classic allylation reaction mediated by zinc powder to synthesis of 3-methyl-3-butene-l-ol （MBOH） in tetrahydrofuran/water. The structure was confirmed by the nu- clear magnetic resonance （IH and 13CNMR）,IR and mass spectrometry （LRMS）. The purity was checked by GC up to 99%. The optimization of conditions to synthesis 3-methyl-3- butene-l-ol was discussed by the molar ratio of reagents, the time, the temperature and other factors. Meanwhile, the syn- thesis of 3-methyl-3-butene-1 -ol from methallyl chloride under a small amount of acetic acid in toluene/water solvent was al- so readily available. The operation was convenient, and it is potential to further applied in industrial production.