合成了4种μ-氧桥联双核金属卟啉,并对包括中间产物在内的几种物质进行表征.同时比较了其对应的合成方法,即一步法和分步法,并就一步法的优越性加以论述.
Four kinds of μ-oxygen bridge binuclear metalloporphyrin were synthesized,and several compounds,including intermediate products and final products,were charaterized by ~1H NMR and FTIR.The two synthetic methods,one-step and fractional step method,were compared simultaneously,and the advantages of one-step method were discussed.