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AlN添加量对BN基复合陶瓷物相组成、微观结构及力学性能的影响
  • ISSN号：0454-5648
  • 期刊名称：《硅酸盐学报》
  • 时间：0
  • 分类：TQ174.75[化学工程—陶瓷工业;化学工程—硅酸盐工业]
  • 作者机构：[1]哈尔滨工业大学材料科学与工程学院,哈尔滨150080
  • 相关基金：国家自然科学基金委创新研究群体（51021002）：国家杰出青年科学基金（51225203）资助项目.
作者： 田卓[1], 贾德昌[1], 段小明[1], 杨治华[1], 周玉[1]
关键词： 氮化硼, 氮化铝, 二氧化硅, 复合陶瓷, 弯曲强度, 断裂韧性, boron nitride, aluminium nitride, silicon dioxide, composite ceramics, flexural strength, fracture toughness
中文摘要：

以BN、SiO2和A1N为原料，采用热压工艺制备出BN-30％SiO2复合陶瓷，研究了A1N添加量对复合陶瓷物相组成、微观组织及力学性能的影响。结果表明：随着A1N的引入，烧结后的复合陶瓷中出现SiAlON相。当材料中AIN加入量小于5％时，可发现有非晶SiO2相。随A1N加入，复合陶瓷弯曲强度和断裂韧性较BN-30％SiO2复合陶瓷均有所提高，并随A1N添加量增加呈先升高后降低趋势，而弹性模量增加并不明显。AIN添加量为5％时，材料弯曲强度和断裂韧性达到最大值（分别为247.0MPa和4.02 MPa·m^1/2），与BN-Si02复合陶瓷相比，分别提高了57.5％和40.6％。

英文摘要：

The BN-based composite ceramics were fabricated with BN, SiO2 and A1N as raw materials by an hot-press sintering process. The effect of A1N content on the phase constitution, microstructure and mechanical properties of the composites was investigated. The results show that SiA1ON can appear in the composites sintered by a hot pressing due to the introduction of A1N. The amorphous SiO2 appears in the composites without A1N or with A1N of 〈 5%. The flexural strength and fracture toughness of the composite, which are greater than those of BN-30%SiO2 composite, firstly increase and then decrease with the increase of AIN. The elastic modulus does not increase. When AIN content is 5%, the flexural strength and fracture toughness are 247.0 MPa and 4.02 MPa.m^1/2, respectively, which are 57.5% and 40.6% greater than those of BN-SiO2 composites.

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期刊信息
  • 《硅酸盐学报》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:中国硅酸盐学会
  • 主编：南策文
  • 地址：北京海淀区三里河路11号
  • 邮编：100831
  • 邮箱：jccsoc@sina.com
  • 电话：010-57811253 57811254
  • 国际标准刊号：ISSN：0454-5648
  • 国内统一刊号：ISSN：11-2310/TQ
  • 邮发代号:2-695
  • 获奖情况:
  • EI　Compendex、CA、SA、PI收录期刊,全国核心期刊,中国期刊方阵“双效”期刊
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  • 美国化学文摘（网络版）,荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊（2004版）,中国北大核心期刊（2008版）,中国北大核心期刊（2011版）,中国北大核心期刊（2014版）,英国英国皇家化学学会文摘,中国北大核心期刊（2000版）
  • 被引量:27713