中文摘要：

利用中温水热技术合成了新型层状磷钒铜多金属氧酸盐（NH3CH2CH2NH3）4[CuV6O8（HPO4）6（PO4）2（H2O）2].4 H2O,采用元素分析、红外光谱、热重分析和X射线单晶结构分析对其进行了表征.结果表明：该化合物属于单斜晶系,C2/c空间群;晶胞参数a=2.0760 nm,b=1.0030 nm,c=2.3784 nm,α=90°,β=101.17°,γ=90°,V=4.8586 nm3,Z=8,R1=0.0719,wR2=0.1432.

英文摘要：

A layered structure compound,（NH3CH2CH2NH3）4[CuV6O8（HPO4）6（PO4）2（H2O）2]·4H2O,was first prepared by hydrothermal synthesis and characterized by elemental analysis,IR,TGA-DSC and single crystal X-raydiffraction.Crystal data：monoclinic,space group C2/c,a=2.076 0 nm,b=1.003 0 nm,c=2.378 4 nm,α=90°,β=101.17°,γ=90°,V=4.8586 nm3,Z=8,R1=0.0719,wR2=0.1432.