FeSiAl 不规则颗粒在酒精溶剂中球磨,制备得到直径为10μm左右厚度为1μm左右的FeSiAl微米片,然后用硅烷偶联剂对微米片表面进行包裹处理。用电子显微镜和 X 射线光谱仪对包裹和未包裹样品做形貌观测和元素分析,并将样品制备成45%(体积分数)的石蜡复合材料,通过矢量网络分析仪测试其在0.1-18 GHz范围内的电磁参数,发现包裹和未包裹样品的复数磁导率曲线基本重合,但包裹后样品的复数介电常数有很明显的下降。微波传输理论计算表明,包裹后样品在L-S波段具有更优越吸波性能。
The irregular FeSiAl particle was used as a raw material for ball milling with alcohol solvent to pro-duce micron-flakes of the diameter and thickness was about 10 μm and 1 μm,and then used silane coupling agent to package the flakes surface.The morphology and the element content of the packaged sample were in-vestigated with SEM and XPS.The frequency-dependent complex permeability of paraffin composites with 45%volume concentration of flakes was measured using the coaxial line method in 0.1-18 GHz frequency range.Af-ter surface modification the complex permittivity of the packaged composite decreased dramatically in the 0.1-5 GHz frequency range,but the permeability wasn’t found obvious change.The calculated microwave re-flectivities indicated that packaged sample had better absorbing performance than unpackaged sample in L-S fre-quency band.