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中文摘要：
采用原位水热合成法，在SiO2-MoO3-TPAOH—Na2O-H2O体系中成功合成了纳米Mo-ZSM-5分子筛，并通过TEM、粉末X射线衍射（XRD）、红外光谱（FT—IR）、紫外可见漫反射（UV-Vis）和紫外拉曼光谱（UV-Ramam）手段对其进行了表征。结果表明，该分子筛粒径为10～30nm，粒度分布均匀。随着Mo含量的增加，纳米Mo-ZSM-5样品的晶胞参数随之增大。此外，FT—IR谱在968cm^-1出现弱吸收峰、UV—Ramam谱在967cm^-1出现吸收峰，并且其强度随着Mo原子含量的增加而增强，充分证明Mo原子进入了纳米Mo—ZSM-5分子筛骨架。
英文摘要：
The nanosized Mo-ZSM-5 was synthesized by hydrothermal method in the SiO2-MoO3-TPAOH-Na2O-H2O system and characterized by TEM, X-ray diffraction （XRD）, FT-IR spectrometer, UV-Vis, UV Raman spectrometer. The results showed that the diameters of synthesized Mo-ZSM-5 particles were uniformly distributed in the range of 10-30 nm. With the Mo content increasing, the cell parameters of the sample increased. Moreover, there was a weak peak at 968 cm^-1 in FT-IR spectrum and a bread peak at 967 cm^-1 in UV-Raman spectrum, and their intensity increased with the Mo content, which fully proved that Mo atoms were introduced into the framework of the ZSM-5 molecular sieve.
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