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透射电镜原位拉伸研究金属材料形变机制
  • ISSN号:1000-6281
  • 期刊名称:《电子显微学报》
  • 时间:0
  • 分类:TB3[一般工业技术—材料科学与工程] O7[理学—晶体学]
  • 作者机构:[1]北京工业大学,固体微结构与性能研究所,北京100124, [2]澳大利亚悉尼大学,机械与机电工程系,新南威尔士2006, [3]中国科学院金属研究所,沈阳材料科学国家联合实验室,辽宁沈阳110016
  • 相关基金:国家自然科学基金资助项目(10776032和50125103); 中国科学院百人计划; 国家重点基础研究发展计划(2009CB623702和2006CB605104); 教育部长江学者奖励计划的资助
中文摘要:

透射电镜原位拉伸方法是研究材料形变机制的一种直观而有效的手段。将拉伸实验与高分辨透射电镜相结合,通过在原子尺度上直接观察,实时地记录应力应变作用下晶体材料微观结构的演变及位错的产生和运动等,直观地揭示材料在弹性及塑性阶段的形变机理。本文将重点回顾近年来作者用透射电镜原位拉伸方法在研究金属材料形变机制方面的工作进展。主要包括纳米金属材料的晶界发射和吸收不全位错、晶粒旋转长大等变形机制,及金属材料在变形过程中的几种可逆形变机制。

英文摘要:

Direct and dynamic atomic level imaging during tensile straining inside a transmission electron microscope(TEM) provides an insight into the deformation processes,which could not be discovered properly by postmortem or ex situ TEM observations.Therefore,in situ TEM observations are of advantage to study the reversible deformation behaviors.Using a combination of in situ tensile straining and high-resolution transmission electron microscopy(HRTEM),the microstructure evolution as well as the nucleation and movement of dislocations upon tensile strain can be recorded in real time and at atomic scale.Based on the intuitive and dynamic observations,the deformation mechanisms in both the elastic and plastic portions could be explored.In this paper,we reviewed several new deformation mechanisms in metallic materials discovered by in situ TEM /HRTEM.A high propensity for the reversibility of the stacking fault was found in nanocrystalline Ni.With the in situ atomic-scale observation,the evidences of the partial dislocation emission from a GB and the absorption of the partial by the original GB were captured.Deformation-induced grain rotation and growth as one of plastic deformation mechanisms in nc materials was revealed by exhibiting the complete process of individual grain rotation and neighboring grain rotation/growth.Reversible deformation twinning was successfully observed in pure,coarse-grained aluminium.By capturing the dynamical process of the twinning and de-twinning at the atomic scale,the physics of the reversible twinning has been revealed.For the abnormal nonlinear elastic deformation behavior of a beta-titanium alloy,HRTEM observations during in situ tensile test revealed new reversible deformation mechanisms:reversible nanodisturbances and reversible movement of homogenously nucleated dislocations.

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期刊信息
  • 《电子显微学报》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:中国物理学会
  • 主编:张 泽
  • 地址:北京市海淀区中关村北二条13号5号楼301
  • 邮编:100190
  • 邮箱:dzxwxb@blem.ac.cn
  • 电话:010-82671519 62565522/3301
  • 国际标准刊号:ISSN:1000-6281
  • 国内统一刊号:ISSN:11-2295/TN
  • 邮发代号:
  • 获奖情况:
  • 曾获《中国科技论文统计源期刊(中国科技核心期刊)》,《中国科学引文数据库(核心库)》来源期刊,中国自然科学核心期刊(无线电电子学、电信技术类...
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  • 被引量:6569