目的:建立香桂化浊胶囊的质量标准。方法:采用薄层色谱(TLC)法鉴别香桂化浊胶囊中的土大黄和肉桂;用气相色谱法对君药广藿香中百秋李醇进行定量分析。结果:定性鉴别分离较好,专属性强;百秋李醇进样量在0.7656~3.8280μg范围内与峰面积积分值呈良好的线性关系(r=0.9999),平均回收率为99.17%,RSD=1.65%(n=6)。结论:所建标准可用于香桂化浊胶囊的质量控制。
OBJECTIVE:To establish the quality standard of Xianggui huazhuo capsules.METHODS:Nepal Dock Root and Cinnamomum cassia in Xianggui huazhuo capsule were identified by TLC;Patchouli alcohol in the principal drug Herba Pogostemonis was analyzed quantitatively by GC.RESULTS:The qualitative identification is well-separated and specific.The linear range of patchouli alcohol was 0.765 6~3.828 0 μg(r=0.999 9) with an average recovery of 99.17%(RSD=1.65%,n=6).CONCLUSION:Established standard is suitable for the quality control of Xianggui huazhuo capsule.