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Characterization of Mo-Si-B Nanocomposite Powders Produced Using Mechanical Alloying and Powder Heat Treatment
  • ISSN号:1005-0302
  • 期刊名称:《材料科学技术学报:英文版》
  • 分类:TG139.8[金属学及工艺—合金;一般工业技术—材料科学与工程;金属学及工艺—金属学] TB383[一般工业技术—材料科学与工程]
  • 作者机构:[1]State Key Laboratory for Mechanical Behaviour of Materials, Xi'anflaotong University, Xi'an 710049, China, [2]School of Materials Science and Engineering Xi'an University of Technology, Xi'an 710048, China
  • 相关基金:This work was supported by the National Natural Science Foundation of China (Grant Nos. 51171149 and 51371141) and the National Science Technology Supporting Program of China (Grant No. 2012BAE06B02).
中文摘要:

有 Mo-12Si-8.5B 的一篇作文的 Mo-Si-B nanocomposite 粉末(在 at.%) 在不同 milling 时间和 powder-to-ball 比率在 milling 条件下面用机械 alloying 被处理。Mo-12Si-8.5B 合金,由瞬间和金属间化合的瞬间 33 Si 和 T2 分阶段执行,它甚至在在 900  °C 的低温度的退火以后形成了。增加退火的温度仅仅改进了各种各样的阶段的 crystallinity。当 milled 和退火的粉末是 hot-pressed sintered 时, Mo-Si-B 合金展出了有细密纹理的微观结构,在的地方 intermetallics 瞬间 3 Si 和 T2 在一个连续瞬间矩阵被散布。

英文摘要:

Mo-Si-B nanocomposite powders with a composition of Mo-12Si-8.5B (in at.%) were processed using mechanical alloying under milling conditions for different milling time and powder-to-ball ratios. The Mo-12Si-8.5B alloy, which consists of α-Mo and intermetallic Mo3Si and T2 phases, was also synthesized by hot-pressed sintering the mechanically alloyed powders under a pressure of 50 MPa at 1600 ℃. The results demonstrated that the sizes and morphologies of the powder particles became gradually refined and uniform by both increasing the milling time and decreasing the powder-to-ball ratio. After 15 h of milling, the powders were completely homogenized at the 1:10 and the 1 : 15 powder-to-ball weight ratios, and the homogenization was accelerated to rapidly stabilize the milling process because of their high milling energy. Annealing the Mo-Si-B milled powders could promote the growth of the intermetallic Mo3Si and the T2 phases, which formed even after low-temperature annealing at 900 ℃. Increasing the annealing temperature only improved the crystallinity of various phases. When the milled and annealed powders were hot-pressed sintered, the Mo-Si-B alloy exhibited a fine-grained microstructure, where the intermetallics Mo3Si and T2 were distributed in a continuous α-Mo matrix.

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期刊信息
  • 《材料科学技术学报:英文版》
  • 中国科技核心期刊
  • 主管单位:中国科协
  • 主办单位:中国金属学会
  • 主编:
  • 地址:中国沈阳文化路72号
  • 邮编:110016
  • 邮箱:
  • 电话:024-83978208
  • 国际标准刊号:ISSN:1005-0302
  • 国内统一刊号:ISSN:21-1315/TG
  • 邮发代号:
  • 获奖情况:
  • 国家“双百”期刊
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  • 被引量:474