以间苯二甲酸为原料,经多步反应合成了化合物5-(8-羟基喹啉-5-偶氮)-1,3-苯二甲酸二乙酯,该化合物与氯乙醇进一步反应得到一种新型偶氮苯(喹啉)化合物,并通过IR、1H NMR对其结构进行了表征。
5-(8-Hydroxyquinoline-5-azo)-1,3-diethyl- phthalate was synthesized through multi-step reaction with isophthalic acid as raw material.Then it reacted with chloride ethanol further to get a new type of azobenzene quinoline compound. The structure of the compound was characterized by IR and 1H NMR.