通过顶空固相微萃取结合气一质联用技术,分析检测中药良姜的挥发性组分,研究萃取时间、萃取温度对良姜挥发性物质数量的影响。结果表明,当萃取时间为35min,萃取温度为60℃时共检出53种化学组分,其中52种物质可鉴别。其主要组分是萜烯类化合物(w=40.238%)、桉树脑(W=23.066%)、α-松油醇(W=8.522%)、β-蒎烯(伽=3.618%)和莰烯(W=3.001%)等。
Headspace solid phase micro-extraction coupling with gas chromatography-mass spectrometry (HS-SPME/GC-MS) was used to analyze volatile compounds of galangal. Effect of extraction time and temperature on the amount of identified compounds was discussed under the optimal SPME conditions :35 min extraction time ,60℃ extraction temperature. 53 kinds of compounds were separa- ted by the gas chromatography and 52 kinds of these can be determined under certain conditions above with the results as follows:the main component was terpenes (40. 238% ), and other compounds of high content were eucalyptol (23. 066% ), p-menth-l-en-8-ol (8. 522% ), 13-pinene ( 3. 618% ), eamphene ( 3. 001% ), and so on.