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Synthesis of Ti2AlC by hot pressing and its mechanical and electrical properties
  • 时间:0
  • 分类:TG11[金属学及工艺—物理冶金;金属学及工艺—金属学]
  • 作者机构:[1]College of Chemistry and Environmental Engineering, Hubei University of Technology, Wuhan 430068, China, [2]State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China
  • 相关基金:Project(50572080) supported by the National Natural Science Foundation of China; Project(SYSJJ2005-04) supported by the Open Foundation of Key Laboratory of Silicate Materials Science and Engineering (Wtthan University of Technology), Ministry of Education
  • 相关项目:Ti-Al-C系陶瓷/TiB2复合材料的制备与界面控制
中文摘要:

高纯净的 Ti2AlN 陶器被热压在 1300 ° C 准备(HP ) Ti/Al/TiN,在 stoichiometric 的粉末分配。sintered 产品用 X 光检查衍射(XRD ) 和 MDI 碧玉被描绘 5.0 软件(材料数据公司,加州利物浦) 。扫描电子显微镜学(SEM ) 和电子探针微量分析(EPMA ) 结合了精力散的光谱学(版本) 被利用调查形态学特征。结果证明那个 Ti2AlN 阶段与靠近、薄片状的结构是开发得好的。谷物与 3 5 μ m, 8 10 μ m 的厚度和伸长的尺寸的尺寸是像板的。Ti2AlN 的密度被测量是 4.22 g/cm3,它到达 97.9% 它的理论价值。Ti2AlN 谷物的分发是同类的。

英文摘要:

High-purity Ti2AIN ceramic was prepared at 1300℃ by hot pressing(HP) of Ti/Ai/TiN powders in stoichiometric proportion. The sintered product was characterized using X-ray diffraction(XRD) and MDI Jade 5.0 software (Materials Data Inc, Liverpool, CA). Scanning electron microscopy(SEM) and electron probe micro-analysis(EPMA) coupled with energy-dispersive spectroscopy(EDS) were utilized to investigate the morphology characteristics. The results show that Ti2AIN phase is well-developed with a close and lamellar structure. The grains are plate-like with the size of 3-5 μm, thickness of 8-10 μm and elongated dimension. The density of Ti2AlN is measured to be 4.22 g/cm^3, which reaches 97.9% of its theory value. The distribution of Ti2AlN grains is homogeneous.

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