以苯并喹啉、氯甲酸乙酯为原料,Ru(PPh3)3Cl2为催化剂,通过C—H活化反应合成了10-乙氧酰基苯并喹啉.产物由熔点、^1H NMR、^13C NMR和IR表征.通过优化合成条件,产物收率可达66%.
10-Acetoxy benzoquinoline was synthesized with benzoquinoline,ethyl carbonochloridate as starting materials,Ru( PPh3)3Cl2as catalyst via C-H activation. The product was characterized by melting point,IR and NMR resonance,and optimized synthetic conditions were also identified and the yield of product can be obtained in 66%.