位置:成果数据库 > 期刊 > 期刊详情页
常温下溶胶-凝胶法制备纳米TiO2及紫外光降解甲基橙性能研究
  • 时间:0
  • 分类:O647.1[理学—物理化学;理学—化学]
  • 作者机构:[1]新余学院新能源科学与工程学院,江西新余338031
  • 相关基金:国家自然科学基金项目(51263021); 江西省教育厅青年基金项目(GJJ11258)
中文摘要:

以钛酸四丁酯为原料,常温下采用溶胶-凝胶法成功制得了纳米二氧化钛粉末,对其制备影响因素进行了研究。经试验结果表明:水和钛酸丁酯的摩尔比是3∶1;冰醋酸与钛酸丁酯的摩尔比是0.5∶1;无水乙醇与钛酸丁酯的摩尔比是20∶1,p H取2-3时凝胶时间达到最佳值。并对试验制得的二氧化钛通过紫外光的照射,会对甲基橙溶液进行分解。在二氧化钛投入量为1.5 g/L,用紫外光照射10 mg/L的甲基橙溶液,4 h后甲基橙的降解率达到了92.9%,在该条件下二氧化钛的光降解效率达到了最高。

英文摘要:

Using tetrabutyl titanate as raw materials,preparation nano titanium dioxide powder by using sol-gel method successfully,the optimum process parameters were discussed in this paper. The test results show that the molar ratio of the water and butyl titanate is 3∶1; The molar ratio of glacial acetic acid and butyl titanate is 0. 5∶1; Anhydrous ethanol and the molar ratio of butyl titanate is 20∶1,pH of 2 - 3. And the test on decomposition of methyl orange solution of titanium dioxide by ultraviolet irradiation. The test results show that titanium dioxide mass is 1. 5 g / L,10 mg / L of methyl orange solution,the degradation of methyl orange rate reached 92. 9% after four hours by using uv irradiation,under the condition of the highest photodegradation efficiency of titanium dioxide.

同期刊论文项目
同项目期刊论文