通过真空感应熔炼、锻造及拔丝工艺制备了成分源于Ni48Ti46Nb3W3(原子分数)的W/NiTi(Nb)形状记忆合金原位自生复合材料,采用X射线衍射仪、扫描电镜、能谱仪及拉伸试验机研究了其微观组织结构与力学性能。结果表明:复合材料丝材中w呈横截面为片状的亚微米级纤维,且沿丝轴向均匀分布在NiTi(Nb)基体中,两组元界面结合良好;该复合材料丝材在室温下平台应力达1.2GPa,并呈现高机械阻尼性能。
An in situ W/NiTi(Nb) shape memory alloy composite with a nominal composition of Ni48 Ti46 Nb3W3 (at. ~) was fabricated by vacuum induction melting, forging and drawing. X-ray diffraction, scanning electron mi- croscope and energy dispersive spectroscopy were employed to analyze the microstructures and tensile testing ma- chine used to investigate the mechanical properties. It is revealed that the microstructure of the composite wire con- sists of tungsten submicro fibers well dispersed in the TiNi(Nb) matrix and aligned along the wire axial direction, with well-bonded interfaces. The composite wire exhibits high plateau stress up to 1.2 GPa and high mechanical damping capacity at room temperature.