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Formation and dissociation of bamboo-like ErD2/ErD3 grains
  • ISSN号:1005-0302
  • 期刊名称:Journal of Materials Science & Technology
  • 时间:2013.11
  • 页码:1101-1103
  • 分类:TS665.1[轻工技术与工程] TB565.1[交通运输工程—水声工程;理学—物理;理学—声学;一般工业技术]
  • 作者机构:[1]Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, China
  • 相关基金:Project supported by the National Natural Science Foundation of China (Grant Nos. 91126001, 11105128, and 51231002). The authors thank Prof. Duanwei He (Institute of Physics, Chinese Academy of Sciences) for the fruitful discussion.
  • 相关项目:反应堆辐照环境下锆合金的损伤机理研究
中文摘要:

A simple and convenient pressure calibration method is developed for a newly designed portable wide-access‘panoramic’ cell. This cell is adapted to angle-dispersive-mode high-pressure in situ neutron diffraction of reactor neutron sources. This pressure calibration method has established a relationship between the cell pressure and the anvil displacement(gasket compression) based on the fixed-point calibration technique. By employing TiZr gasket with a thickness of3 mm and WC anvil with a culet of 4 mm diameter, the average anvil displacements are 1.31 mm and 2.22 mm for Bi phase transitions(2.55 GPa and 7.7 GPa), and 1.85 mm for Ba phase transitions(5.5 GPa), respectively. In this pressure range, the pressure increases quickly with decreasing gasket thickness, and undergoes a linear increase with the anvil displacement.By extrapolating the calibration curve, the cell pressure will achieve 10 GPa when the anvil displacement is around 2.5 mm.

英文摘要:

A simple and convenient pressure calibration method is developed for a newly designed portable wide-access 'panoramic' cell. This cell is adapted to angle-dispersive-mode high-pressure in situ neutron diffraction of reactor neutron sources. This pressure calibration method has established a relationship between the cell pressure and the anvil displace- ment (gasket compression) based on the fixed-point calibration technique. By employing TiZr gasket with a thickness of 3 mm and WC anvil with a culet of 4 mm diameter, the average anvil displacements are 1.31 mm and 2.22 mm for Bi phase transitions (2.55 GPa and 7.7 GPa), and 1.85 mm for Ba phase transitions (5.5 GPa), respectively. In this pressure range, the pressure increases quickly with decreasing gasket thickness, and undergoes a linear increase with the anvil displacement. By extrapolating the calibration curve, the cell pressure will achieve 10 GPa when the anvil displacement is around 2.5 ram.

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期刊信息
  • 《材料科学技术学报:英文版》
  • 中国科技核心期刊
  • 主管单位:中国科协
  • 主办单位:中国金属学会
  • 主编:
  • 地址:中国沈阳文化路72号
  • 邮编:110016
  • 邮箱:
  • 电话:024-83978208
  • 国际标准刊号:ISSN:1005-0302
  • 国内统一刊号:ISSN:21-1315/TG
  • 邮发代号:
  • 获奖情况:
  • 国家“双百”期刊
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  • 被引量:474