位置:成果数据库 > 期刊 > 期刊详情页
热变形(Nd,Pr)-Fe-Nb-B磁体取向度及矫顽力机制研究
  • ISSN号:0258-7076
  • 期刊名称:《稀有金属》
  • 时间:0
  • 分类:V252.4[一般工业技术—材料科学与工程;航空宇航科学与技术—航空宇航制造工程;航空宇航科学技术]
  • 作者机构:宁波大学材料科学与化学工程学院,宁波市新型功能材料及其制备科学重点实验室,浙江宁波315211
  • 相关基金:国家自然科学基金项目(51174121,51274125); 浙江省重点科技创新团队项目(2012R10016-08); 宁波大学王宽诚幸福基金项目资助
中文摘要:

采用X射线衍射(XRD)、扫描电镜(SEM)分析了热变形Nd_(10.5)Pr_(2.5)Fe_(80)Nb_1B_6磁体断口等显微组织,并用磁滞回线仪测量了磁体的磁性能,系统研究了磁体显微组织、磁性能与取向度的变化规律。估算了250~380μm和〈250μm Nd_(10.5)Pr_(2.5)Fe_(80)Nb_1B_6粉、变形量60%的热变形磁体等效易磁化轴与热变形压力方向夹角α,随α从26.0°降至9.1°,磁体密度从7.04 g·cm~(-3)增加至7.49 g·cm-3,M_r/M_s(M_r为剩余磁化强度,Ms为饱和磁化强度)从0.78增大到0.91,磁能积持续增加,矫顽力先从1346 k A·m~(-1)增加至1499 k A·m~(-1),然后矫顽力下降到1216 k A·m~(-1),矫顽力增加的原因是磁体单位体积内磁性主相体积分数增加导致对矫顽力的贡献增大,更多的等轴晶参与热变形、晶粒发生碎化、晶粒尺寸细化;随着α的继续降低,热变形磁体的剩磁、矫顽力将分别进一步增加、减小,矫顽力减小的原因是片状晶的比例增加,片状晶的晶粒尺寸增大,单畴晶粒占总磁畴晶粒比例减小,片状晶出现退磁场。实验统计热变形Nd_(10.5)Pr_(2.5)Fe_(80)Nb_1B_6矫顽力与等效平均晶粒尺寸的关系拟合曲线为Hci=1523.3786+0.3280D-0.0031D2,矫顽力随等效平均晶粒尺寸的增大而降低。

英文摘要:

Ndl0.5Pr2.5Fe80Nb1B6 magnets were die-upset at height reduction of 60%, with compacts of 250 - 380 μm or 〈 250 μm particles. The magnets were detected by X ray diffraction (XRD) , scanning electron microscopy (SEM) , and measured by a hystere- sis loop tester at room temperature. The microstructures, magnetic properties, orientation degree and coercive force mechanism were studied and discussed, α, the angle between the equivalent easy magnetization axis of the magnets and the die-upset pressure direc- tion, was calculated. As α decreased from 26.0° to 9.1°, the density of the magnets increased from 7.04 to 7.49 g.cm-3 , Mr/Ms (Mr, MS was the remnant magnetization, and the saturation one, respectively) was from 0.78 to 0.91, the magnetic energy increased, but the coercive force climbed first from 1346 to 1499 kA m-1, and then reduced to 1216 kA m-1. The climbing reasons were that more grains of the magnetic matrix phase in unit volume contributed to the coercive force, and more equiaxed grains joined the die-up- set process and were broken. And the reducing reasons were that more and larger lamellae grains were obtained while the bigger demag- netizing fields of the grains appeared, and the proportion of single-domain grains in magnets decreased. The curve fitting between coer- cive force of Nd10.5Pr2.5Fe80Nb1B6 die-upset magnets and their equivalent average grain size D, was Hci = 1523. 3786 + 0. 3280D - 0. 0031D2. And the coercive force reduced as the grain size increased.

同期刊论文项目
同项目期刊论文
期刊信息
  • 《稀有金属》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:北京有色金属研究总院
  • 主编:屠海令
  • 地址:北京新街口外大街2号
  • 邮编:100088
  • 邮箱:xxsf@grinm.com
  • 电话:010-82241917 62014832
  • 国际标准刊号:ISSN:0258-7076
  • 国内统一刊号:ISSN:11-2111/TF
  • 邮发代号:82-167
  • 获奖情况:
  • 中文核心期刊,冶金工业类核心期刊,中国科技论文统计源期刊
  • 国内外数据库收录:
  • 俄罗斯文摘杂志,美国化学文摘(网络版),荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),中国北大核心期刊(2000版)
  • 被引量:13688