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凝胶注模成型用锆钛酸铅陶瓷浆料流变特性研究
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  • 分类:TM28[电气工程—电工理论与新技术;一般工业技术—材料科学与工程]
  • 作者机构:[1]南华大学化学化工学院,湖南衡阳421001, [2]南华大学经济管理学院,湖南衡阳421001
  • 相关基金:国家级大学生创新创业训练计划基金资助项目(201510555004); 湖南省教育厅优秀青年基金资助项目(15B200); 南华大学博士科研启动基金资助项目(2014XQD04); 国家自然科学基金资助项目(51574152)
中文摘要:

分别采用聚丙烯酸铵和海因环氧树脂为分散剂和凝胶剂,制备锆钛酸铅(PZT)压电陶瓷浆料,研究了分散剂含量、球磨时间、固相含量以及树脂含量等因素对浆料流变性能的影响,结果表明,当分散剂加入量为0.6%、球磨时间为24 h及固相体积含量为55.0%时,浆料流变特性最佳.浆料粘度随着树脂含量增加而增大,但即使树脂含量高达25.0%,浆料流动性依然能较好满足浇注成型的需求.

英文摘要:

The lead zirconate titanate( PZT) suspensions were prepared using the ammonium polyacrylate and Hydantion epoxy resin as the dispersant and the gelling agent,respectively.The effects of the dispersant concentrations,the milling time,the solid loading and the epoxy resin content on the rheological properties of the PZT suspensions were systematically investigated.The results show that the rheological property of the PZT suspesion was the best when the dispersant concentration,the milling time and the solid loading were0. 6%,24 h and 55.0%,respectively. Although the viscosities of the suspensions increasedwith the increase of the epoxy resin content,the fluidity of the suspension even with 25.0%resin was still good for the requirement of the gelcasting process.

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