试图学习 Monochasma savatierii Franch 的化学成分。化学成分被列层析与硅石胶化孤立并且反复净化了的方法, Rp-C18, Sephadex LH-20 并且由红外, MS 和 NMR 识别了。结果和八混合物作为 7 被获得并且识别, 8-dehydroboschnialactone (1 ) , argyol (2 ) , liquirtigenin (3 ) , -sitosterol (4 ) , p-hydroxycinnamic 酸(5 ) , 2-hydroxy-4-methoxybenzonic 酸(6 ) , p-hydroxyphenylethanol (7 ) , protocatechuic 酸(8 ) 。结论化合物 1 第一次从生来的来源被获得,其它第一次从这植物被孤立。
AIM: To study the constituents in the roots of Achyranthese bidentata Bl. METHODS: D-101 porous polymer resin column, normal-phase silica gel column chromatography, revised-phase medium pressure column chromatography, Sephadex LH-20 and prep-HPLC were used for the separation, and spectroscopic techniques were employed for the identification of the isolated compounds. RESULTS: Five saponins were isolated and elucidated as achyranthoside C (1), achyranthoside D (2), chikusetsusaponin Ⅳ (3), ginsenoside Ro (4) and zingibroside R1 (5). CONCLUSION: Compound 1 was obtained from natural source for the first time, and compound 3 was reported from the family of Amaranthaceae for the first time.