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胜利褐煤水热解聚物中正构烷基环戊烷的富集与分析
  • ISSN号：1004-7077
  • 期刊名称：枣庄学院学报
  • 时间：2015.4.20
  • 页码：35-38
  • 分类：TQ536[化学工程—煤化学工程]
  • 作者机构：[1]枣庄学院化学化工与材料科学学院,山东枣庄277160, [2]中国石油大学化工学院,山东青岛266555, [3]中国矿业大学化工学院,江苏徐州221116
  • 相关基金：国家973计划课题（项目编号：2011CB201302）; 国家自然科学基金重点项目（项目编号：20936007）;国家自然科学基金神华集团煤炭联合基金重点项目（项目编号：51134021）;国家自然科学基金（项目编号：51074153;21276268和21206187）; 国家自然科学基金委员会创新研究群体科学基金（项目编号：51221462）; 中日战略合作项目（项目编号：2013DFG60060）; 枣庄学院博士科研基金
  • 相关项目：煤直接液化过程中活性氢的形成及其对加氢液化的作用机理
作者： 王雪|任崇桂|宗志敏|魏贤勇|
关键词： 褐煤, 分子煤化学, 长链烷基环戊烷, 微固液萃取1, lignite, molecular coal chemistry, long-chain alkylcyclopentane, micro-solid / liquid extraction
中文摘要：

胜利褐煤在240oC下的Na OH/水中热溶2 h得到水热解聚物（TW）.向TW中加入盐酸使其形成微固相-液相状态,然后在超声波辐射下依次用石油醚、环己烷、二硫化碳和苯对TW进行分级萃取获得萃取物1到4（E1到E4）.用气相色谱/质谱联用（GC/MS）在E4中检测到了8种偶碳长链烷基环戊烷（C20-34）,它们可能是煤中重要的生物标志物.温和水热解聚结合微固液萃取是分析低阶煤中有机质的有效方法.

英文摘要：

Hydrothermal depolymerization（ HTD） of Shengli lignite was carried out at 240 oC for 2 h to obtain the thermally soluble fraction（ TW）. TWwas transformed into micro- solid phase by adding a proper amount of hydrochloric acid,and then fractionally extracted with petroleum ether,cyclohexane,carbon disulfide and benzene under ultrasonic radiation to offer the extracts 1 to 4（ E1 to E4）. 8 long- chain alkylcyclopentanes with even carbon number,which could be a class of important biomarkers,were detected in E4 by gas chromatography / mass spectrometry（ GC / MS）. Combination of mild HTD and micro-solid / liquid extraction is an effective method to analyze organic substance in low- rank coals.

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晋城15号无烟煤的温和氧化
晋城15号无烟煤的温和氧化
晋城15号无烟煤的温和氧化
方便、有效的方法合成2-氨基-1,3-二氰基-4-芳基-5,6,7,8,9,10,11,12,13,14-十氢苯并[12]轮烯衍生物
方便、有效的方法合成2-氨基-1,3-二氰基-4-芳基-5,6,7,8,9,10,11,12,13,14-十氢苯并[12]轮烯衍生物
方便、有效的方法合成2-氨基-1,3-二氰基-4-芳基-5,6,7,8,9,10,11,12,13,14-十氢苯并[12]轮烯衍生物
煤基多孔碳孔隙逾渗演化过程及结构特征
基于CFD的Falcon分选机内部流场测试
木质素的结构研究与应用
基于DEM的筛面与物料特性在筛分过程中协同作用的研究
高压电脉冲技术对废弃电路板的破碎研究
高剂量亚铁Fenton反应及形成次生铁矿物的特性
Stiffness identification of four-point-elastic-support rigid plate
Comparison of coal separation characteristics based on different separating approaches in dry coal beneficiation flowsheet
Improvement for design of beam structures in large vibrating screen considering bending and random vibration
Dynamic analysis of new type elastic screen surface with multi degree of freedom and experimental validation
基于高压电脉冲破碎废弃电路板粒度分形特性
MOx颗粒活性炭镀层粒子电极对苯酚的电催化降解特性
期刊信息
  • 《枣庄学院学报》
  • 主管单位:山东省教育厅
  • 主办单位:枣庄学院
  • 主编：曹胜强
  • 地址：山东省枣庄市北郊
  • 邮编：277160
  • 邮箱：xyxb@uzz.edu.cn
  • 电话：0632-3786743
  • 国际标准刊号：ISSN：1004-7077
  • 国内统一刊号：ISSN：37-1431/Z
  • 邮发代号:
  • 获奖情况:
  • 中国学术期刊（光盘版）检索与评价规范执行优秀期刊
  • 国内外数据库收录:
  • 被引量:1714