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中文摘要：
合成了一种新型的稀土配合物Eu0.5Tb0.5（TTA）3Bipy，并采用原位乳液聚合法制备了Eu0．5Tb0.5（TTA）3Bipy／PMMA稀土聚合物材料。利用红外光谱仪（IR）、电子探针X射线能谱仪等对稀土聚合物发光材料的结构进行表征，并利用扫描隧道电子显微镜（SEM）、荧光光谱仪（FS）等分别研究了该发光材料的微观形貌，探讨了其发光性能。结果表明，Eu0.5Tb0．5（TTA）3Bipy／PMMA仍保持Eu0.5Tb0.5（TTA）2Bipy原有的发光特性；在365nm紫外光的激发下，产生发光峰在612nm附近、谱线带宽为10．4nm的红光发射，发光亮度高，色纯度高，是性能优良的稀土聚合物发光材料。
英文摘要：
In this paper, Eu0.5Tb0.5（TTA） 3 Bipy was synthesized and Eu0.5 Tb0.5（TTA） 3 Bipy/PMMA was prepared by in-situ polymerization. The structure of Eu0.5Tb0.5（TTA）3Bipy/PMMA was characterized by FT-IR spectra. Microscopic morphology and photoluminescent properties were investigated by SEM photographs and fluorescence spectras. The results indicated that Eu0.5Tb0.5（TTA）3 Bipy/PMMA could emit mostly characteristic fluorescence of europium ion and intense red fluorescence with peak wavelength at 612nm and bandwidth of 10.4 nm（purity：0. 9908） under UV excitation at 365nm. It was demonstrated that Eu0.5Tb0.5（TTA）3Bipy/PMMA was an excellent red photoluminescent rare-earth polymer material.
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