以铝粉、AlCl3·6H2O和水为原料,通过调整原料配比、反应和陈化的温度和时间,经蒸发、结晶,制成了组成为Al24O11(OH)44Cl6的氯化二十四聚铝(Al24)。采用XRD和化学分析对其进行了初步表徵。
A novel ventiquattro-meric polyaluninium chloride, Al24O11(OH)44Cl6 was prepared by using aluminium powder, AlCl3·6H2O and water as reactants, adjusting the recipe, reacting and aging temperature and time, and evaporating and crystallizing. The result product was characterized by XRD and chemical analysis.