欢迎您！东篱公司
退出
-
申报数据库
-
立项数据库
-
成果数据库
-
项目获奖数据库
中文摘要：
以醋酸锌（Zn（CH，COO）2·2H20）和氨水（NH，·H20）为反应物，对比运用微通道和搅拌釜为反应器时所得产物氧化锌形貌的差别。运用同轴环管微通道作为反应器经过水热过程合成一种直径在0.5-lμm，长度在20-30lμm左右新型的棒状氧化锌材料。结果表明，以搅拌釜为反应器得到的产物为不均匀的纳米颗粒，经过水热过程后转变成为直径在1μm左右的均匀星状结构。以在线高速照相机来观察液体在微通道中的流动状态，发现其为均匀的层流流动，讨论运用微通道合成氧化锌的成核和生长机理。
英文摘要：
A microfluidic channel reactor and a stirring reactor were introduced to synthesize ZnO particles by using Zn（CH3COO ）2.2H20 dissolved in ethylene glycol and ammonia liquor solution as feedstocks. The results showed that after the hydrothermal treatment, the products synthesized by microfluidic channel reactor were rod-liked ZnO particles with a length of 20-30 μm and a diameter of 0.5-1 μm. When Zn（CH3COO）_2. 2H_2O was dropped in the ammonia liquor solution into a stirring reactor, the morphology of the products was nonuniform nano-particles , and it changed into starliked structure with a diameter of 1 μmafter thehydrothermal treatment. To observe the fluid flow in the microchannel reactor, an online high-speed camera system was used. The images showed that the flow in the channel was a laminar flow. The mechanism of zinc oxide nucleation and growth was proposed.
同期刊论文项目
同项目期刊论文
Controllable Preparation of SiO2 Nanoparticles Using a Microfiltration Membrane Dispersion Microreac
Development of a gas-liquid microstructured system for oxidation of hydrogenated 2-ethyltetrahydroan
Kinetics research on fast exothermic reaction between cyclohexanecarboxylic acid and oleum in micror
Preparation and ion exchange properties of egg-shell glass beads with different surface morphologies
Iron Phosphate Prepared by Coupling Precipitation and Aging: Morphology, Crystal Structure, and Cr(I
Extraction-Derived Self-Organization of Colloidal Photonic Crystal Particles within Confining Aqueou
One-step synthesis of pH-sensitive poly(Acrylamide-co-Sodium Acrylate) beads with core-shell structu
Controlled stimulation-burst targeted release by smart decentered core-shell microcapsules in gravit
Preparation and the hydrogenation performance of a novel catalyst-Pd nanoparticles loaded on glass b
Synthesis of Titania-Silica Core-Shell Microspheres via a Controlled Interface Reaction in a Microfl
In situ preparation of Pd/Al2O3-SiO2 composite microspheres by combining a sol-gel process and preci
Preparation of Highly Dispersed and Small-Sized ZnO Nanoparticles in a Membrane Dispersion Microreac
Process intensification of catalytic hydrogenation of ethylanthraquinone with gas-liquid microdisper
Preparation of Pseudoboehmite with a Large Pore Volume and a Large Pore Size by Using a Membrane-Dis
A novel microfluidic approach for monodispersed chitosan microspheres with enhanced autofluorescence
Hydration of acrylonitrile to produce acrylamide using biocatalyst in a membrane dispersion microrea
A novel microfluidic approach for preparing chitosan-silica core-shell hybrid microspheres with cont
Size Control and Catalytic Activity of Highly Dispersed Pd Nanoparticles Supported on Porous Glass B
Controllable microfluidic production of gas-in-oil-in-water emulsions for hollow microspheres with t
Microfluidic preparation of chitosan microspheres with enhanced adsorption performance of copper(II)
Preparation of 10 mu m scale monodispersed particles by jetting flow in coaxial microfluidic devices
Preparation and Carbon Dioxide Separation Performance of a Hollow Fiber Supported Ionic Liquid Membr
Continuous Ammonium Silicofluoride Ammonification for SiO2 Nanoparticles Preparation in a Microchemi
Free radical polymerization of butyl acrylate in monodispersed droplets: Comparison between two heat
Controllable Preparation of Poly(butyl acrylate) by Suspension Polymerization in a Coaxial Capillary
Preparation of Mesoporous ZnO Microspheres through a Membrane-Dispersion Microstructured Reactor and
One-step microfluidic approach for controllable production of gas-in-water-in-oil (G/W/O) double emu
Microfluidic production of porous chitosan/silica hybrid microspheres and its Cu(II) adsorption perf
Beckmann rearrangement of cyclohexanone oxime in a microchemical system: The role of SO3 and product
Nano-gel containing thermo-responsive microspheres with fast response rate owing to hierarchical pha
Novel cationic pH-responsive poly(N,N-dimethylaminoethyl methacrylate) microcapsules prepared by a m
Lattice-Boltzmann method for the simulation of multiphase mass transfer and reaction of dilute speci
Direct measurement of the differential pressure during drop formation in a co-flow microfluidic devi
Experimental Study on Dynamic Interfacial Tension with Mixture of SDS-PEG as Surfactants in a Coflow
Controllable preparation of nanoparticle-coated chitosan microspheres in a co-axial microfluidic dev
Liquid-liquid flow and mass transfer characteristics in micro-sieve array device with dual-sized por
期刊信息
位置：