在控制法向载荷分别为20、50和80 N,位移幅值分别为80、150和200μm的两种不同环境下,以Si3N4陶瓷球/Inconel690平面接触的方式,在PLINT高温微动试验机上进行微动腐蚀试验,循环次数为2×104。结果表明:在滑移区,当载荷、位移幅值一定时,相同温度联氨溶液中的稳态摩擦因数比其在蒸馏水中高;稳态摩擦因数随溶液的温度增加而增加;磨损体积随溶液温度增加而增加。Inconel 690在联氨溶液摩擦过程中,磨损程度除受到位移幅值、荷载影响以外,温度对磨损体积有显著影响。温度的增加即降低溶液的溶解氧又促进联胺与溶解氧的吸收反应,起到降低氧化腐蚀的作用。在蒸馏水中Inconel 690合金材料的磨损机制主要为磨粒磨损和剥层,而在联氨溶液中其磨损机制主要为裂纹伴随磨粒磨损和剥层。
The friction and wear behaviors of Inconel 690 flat against Si3Ni4 ball were investigated using a hydraulic fretting test rig equipped with a liquid container device. The loads of 20-80 N, reciprocating amplitudes of 80-200 μm and two different environments (distilled water and hydrazine solution at temperatures from 25 to 90 ℃) were selected. The results show that the ratio of Ft/Fn is lower in distilled water than that in hydrazine solution at the same temperature in the slip regime. Both the ratio of Ft/Fn and wear volume gradually increase with increasing medium temperature under the given normal load and displacement amplitude. Besides the displacement amplitude and load, temperature also plays an important role for wear behavior of Inconel 690 material. The increase of temperature could reduce the concentration of dissolved oxygen, and promote the absorption reaction of hydrazine and dissolved oxygen. As a result, the oxidative corrosion rate is obviously lowered. Abrasive wear and delamination wear are the main mechanisms of Inconel 690 in distilled water. However, in hydrazine solution the cracks accompanied by abrasive wear and delamination wear are the main mechanisms.