以金属氧化物和蔗糖为原料,经混合球磨,高温碳热还原制备Sn—Co—M—C(M=Zn,Fe)复合负极材料.采用XRD、SEM测试样品结构,观察样品形貌.电化学性能测试表明,Sn—Co—Zn—C电极首次嵌锂比容量571mAh·g^-1,45次循环后比容量369mAh·g^-1,其比容量和循环寿命好.
The anode materials of Sn-Co-M-C (M--Zn, Fe) composites were prepared by carbothermal re- duction method from metal oxides and sucrose in N2 atmosphere. Their structural and electrochemical proper-ties were studied by XRD, SEM and charge-discharge test. Among them, the Sn-Co-Zn-C composite showed higher specific capacity and good cycle performance. The initial special discharge capacity of 571 mAh·g^-1 could be obtained, while 369 mAh·g^-1 was still kept after 45 cycles.