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取代基酞菁铜的合成与表征
  • ISSN号：1674-0874
  • 期刊名称：山西大同大学学报(自然科学版)
  • 时间：2011
  • 页码：30-33
  • 分类：O631.1[理学—高分子化学;理学—化学]
  • 作者机构：[1]运城学院应用化学系,山西运城,044000, [2]东北师范大学化学学院,吉林长春130012
  • 相关基金：国家自然科学基金资助项目[61006034]; 山西省青年基金项目[2010021010-3]; 运城学院院级重点项目[975175]; 东北师范大学校内博士后项目[111900026]
  • 相关项目：一类具有1.5微米波长的近红外材料的合成及性质研究
作者： 夏道成|姚纪欢|韩双|马会宣|刘慧景|
关键词： 酞菁, 酞菁锌, 合成, 表征, phthalocyanine, phthalocyanine zinc, synthesis, characterization
中文摘要：

首次使用苯二甲腈和硫酸锌反应合成新型的八取代基酞菁锌.合成方法：苯二甲腈和硫酸锌在DMF中搅拌恒温加热,并加入适量的催化剂1,8-二氮杂-双环（5,4,O）十一碳烯-7（DBU）,反应完毕后,得到目标化合物.通过对产物进行红外、紫外可见光谱、荧光和X-RD的测试,表征其结构,从而证实产物就是目标化合物.

英文摘要：

In this article,we first take phthalonitrile and ZnSO4 as the starting reactants to prepare octa-substituted phthalocyanine zinc.The mixture of phthalonitrile and ZnSO4were used as precursors to synthesis octa-substituted phthalocyanine zinc which was generated by cyclotetramerisation in the presence of 1,8-diazabicyclo undec-7-ene（DBU）.At last,the compound was characterized by infrared,fluorescence and UV-visible spectrum and atomic absorption,proving its structure.Thus it confirmed that the product was the target compound.

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一类具有1.5微米波长的近红外材料的合成及性质研究
期刊论文 40
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期刊信息
  • 《山西大同大学学报：自然科学版》
  • 主管单位:山西大同大学
  • 主办单位:山西大同大学
  • 主编：郝临山
  • 地址：山西省大同市御河桥东
  • 邮编：037009
  • 邮箱：dtxblk@163.com
  • 电话：0352-7665396 7563252
  • 国际标准刊号：ISSN：1674-0874
  • 国内统一刊号：ISSN：14-1344/N
  • 邮发代号:
  • 获奖情况:
  • 国内外数据库收录:
  • 被引量:2280