中文摘要：

以间苯二甲醛、5,5-二甲基-3-对甲苯基氨基环己-2-烯酮和季酮酸为原料,在醋酸和N,N-二甲基甲酰胺（DMF）混合溶剂（体积比2∶1）中,通过微波辅助的多组分反应一步合成标题化合物.结构经红外光谱、核磁共振和元素分析得以确证,并通过单晶X射线衍射进一步确证.该晶体属于三斜晶系,空间群P-1,a=1.16215（14）,b=1.33902（16）,c=1.47823（19）nm,α=96.226（2）°,β=94.729（2）°,γ=106.956（3）°,Mr=720.83,V=2.1716（5）nm3,Dc=1.102g/cm3,Z=2,μ（MoKα）=0.073mm-1,F（000）=764.晶体结构用直接法解出,使用全矩阵最小二乘法对原子参数进行修正,最后的偏离因子R=0.0981,Rw=0.1263.

英文摘要：

The title compound has been synthesized via a green microwave-assisted one-pot reaction of isophthalaldehyde with 3-（p-tolylamino）-5,5-dimethylcyclohex-2-enone and tetronic acid in glacial acetic acid （HOAc） and N,N-dimethylformamide （DMF）, and its structure was determined by monocrystalline X-ray diffraction. The crystal is triclinic, space group P-1 with a 1.162 15（14）, b=1.339 02（16）, c=1.478 23（19） nm,α=96.226（2）°, β=94.729（2）°γ= 106. 956（3）°, Mr=720. 83, V=2. 171 6（5） nm^3, Dc=1. 102 g/cm^3, Z=2, μ （Mo Ka）=0. 073 mm^-1 ,F（000）=764. The structure was solved by direct methods and refined by the full-matrix method of least-squares to the final R=0. 098 1, R=0. 126 3.