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中文摘要：
采用硫代乙酰胺（TAA）、三氯化铁和四氯化铟为原料,超临界水为反应介质,用简单的一步法成功地合成出了FeIn2S4纳米颗粒。利用粉末X射线衍射（XRD）、扫描电子显微镜（SEM）以及透射电子显微镜（TEM）等手段对产物进行了表征。实验结果表明,所得产物为立方相的、面心晶格结构的FeIn2S4,电镜结果显示FeIn2S4纳米颗粒具有片状形貌,颗粒大小在50-100 nm之间,并具有较好的分散性。
英文摘要：
Crystalline FeIn2S4 nanoparticles were successfully synthesized by a simple and one-step way, using thioacetamide （TAA）, trichloride iron and tetrachloride indium as raw materials, supercritical water as reaction medium. The products were characterized by powder X-ray diffraction （XRD）, field-emission scanning electron microscopy （SEM） and transmission electron microscopy （TEM）. The XRD results show that the obtained Feln2S4 had cubic structure and a face-centered lattice. The microscopy images show that the synthesized FeIn2S4 particles were in sheet shape and exhibited weak agglomeration with the size ranging from 50 nm to 100 nm.
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