利用熔模铸造的方法制备了铸造Ti-6Al-4V合金试样,通过金相、电子探针、显微硬度测试等技术研究了铸造钛合金表面α层的组织和形成机理。结果表明,铸造钛合金试样表面均形成了α层,显微组织特征为呈"网篮"状排列的粗大片状α相组织。α层形成机理主要与型壳材料中间隙氧原子和碳原子向合金基体扩散有关。显微硬度测试得到的α层深度略大于金相结果。为完整去除α层,以硬度测试的结果更为可靠。
The ingot of Ti-6Al-4V alloy was prepared by investment casting.Microstructure and formation mechanism of α-case in the surface layer of the ingot were investigated by optical microscope(OM),electron probe micro-analyzer(EPMA) and Vickers hardness testing.The results show that the α-case covers the whole surface of the sample,and the microstructure of the α-case features a coarse plate-shaped structure which is ranked as basketweave.The formation mechanism of α-case is associated with the diffusion of interstitial oxygen and carbon atoms in the shell material toward matrix alloy.Depth of α-case obtained from micro-hardness testing is slightly deeper than that observed by OM.More reliable results come from the micro-hardness testing for removing the α-case completely.