以钛酸四正丁酯((C4H9O)4Ti)水解沉淀的钛羟基氧化物和硝酸锶(Sr(NO3)2)为反应原料,以氢氧化钾(KOH)为矿化剂,以乙二醇((HOCH2)2)为溶剂,经200℃溶剂热反应得到了由纳米颗粒自组装形成的SrTiO3片状纳米结构。分别用XRD、SEM、TEM表征SrTiO3粉体的物相结构和微观形貌。通过光催化降解罗丹明B(RhB)对比研究了乙二醇溶剂热合成的纳米颗粒自组装SrTiO3片状纳米结构和水热合成的SrTiO3粉体的光催化性能,结果表明,乙二醇溶剂热合成的SrTiO3自组装片状纳米结构具有更加优异的光催化性能。
Strontium titanate (SrTiO3) nanosheets self-assembled by nanoparticles were successfully synthesized by ethylene glycol solvothermal reaction route with titanium oxide hydroxyl as reaction materials and potassium hydroxide (KOH) as mineralizer at 200℃. The composition and morphology of the synthesized powders were investigated using XRD, SEM and TEM. The photocatalytic activities of the samples synthesized by hydrother- mal and solvothermal method were studied through recording the degradation of Rhodamine B (RhB) in UV. The result shows that the SrTiO3 self-assembly nanosheets perform better photocatalytic activities.