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(Pb,Sr)Nb2O6-NaNbO3薄膜的制备与介电性能研究
  • ISSN号:0258-7076
  • 期刊名称:《稀有金属》
  • 时间:0
  • 分类:TM536[电气工程—电器]
  • 作者机构:[1]北京有色金属研究总院先进电子材料研究所,北京100088, [2]北京有色金属研究总院智能传感功能材料国家重点实验室,北京100088
  • 相关基金:国家自然科学基金项目(51107005,51477012)资助
中文摘要:

采用脉冲激光技术(PLD)在p+-Si上沉积了(Pb,Sr)Nb2O6-Na Nb O3介质薄膜,介质薄膜在氧化气氛下进行不同温度的热处理,进行光刻图形化、磁控溅射沉积电极之后,形成Al/p+-Si/(Pb,Sr)Nb2O6-Na Nb O3/Au结构的MIM(金属-绝缘体-金属)电容器。通过X射线衍射(XRD)、原子力显微镜(AFM)和高分辨透射电子显微镜(HRTEM)对介质薄膜的微观形貌及结构进行分析。通过测试不同温度热处理后薄膜电容器的I-V和C-V电学特性,研究了不同温度热处理对薄膜电容器漏电流密度、电容、介电损耗及物相的影响,并对电容器电容和损耗的偏压特性进行了分析,结果表明,800℃热处理能显著提高薄膜的介电常数并降低漏电流密度。在偏压为-1 V,频率为1 k Hz的测试环境下,其介电常数为33,漏电流密度约为4.104×10-9A·cm-2,满足微电子领域内对漏电流小于1×10-8A·cm-2的要求;对薄膜电容器特性曲线拟合后得到其二次项电压系数为188,符合国际半导体技术蓝图(ITRS)对未来MIM电容提出的要求,具有良好的应用前景,是制备无机薄膜电容器理想的介质材料。

英文摘要:

(Pb, Sr)Nb206-NaNbO3 dielectric thin films were fabricated by pulsed laser deposition (PLD) technology on p +-Si, The dielectric film was annealed at different temperatures in oxygen atmosphere. Metal insulator metal(M1M) capacitorwith A1/p + -Si/( Pb, Sr) Nb2O6-NaNbO3/Au structure was fabricated after patterning the film in photolithography and preparing electrodes by magnetron sputtering. The microscopic surface topography and surface roughness were studied by X-ray diffraction(XRD) , atomic force microsco- py(AFM) and high resolution transmission electron microscope (HRTEM). The 1-V electrical characteristics and C-V characteristics of MIM capacitor were studied, respectively, the effects of annealing temperature on leakage current density, capacitance, dielectric loss and phase of the MIM capacitor were investigated, furthermore, the bias characteristics of capacitance and dielectric loss were studied, and dielectric constant increased and leakage current density decreased when the film was annealed at 800 . When it was calculated at - 1 V in 1 kHz, the dielectric constant was 33 and the leakage current density was about 4. 104 × 10^-9A·cm^-2, which met the re- quirements for the leakage current density of less than 1 × 10^ -8 A·cm 2 in the field of microelectronics. The quadratic voltage coeffi- cientwas 188 after fitting curve, which met the requirements for the future MIM capacitor released by international technology roadmap for semiconductors (ITRS), and (Pb, Sr)Nb2 O6-NaNbO3 was desirable dielectric material forinorganic thin film capacitor.

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期刊信息
  • 《稀有金属》
  • 中国科技核心期刊
  • 主管单位:中国科学技术协会
  • 主办单位:北京有色金属研究总院
  • 主编:屠海令
  • 地址:北京新街口外大街2号
  • 邮编:100088
  • 邮箱:xxsf@grinm.com
  • 电话:010-82241917 62014832
  • 国际标准刊号:ISSN:0258-7076
  • 国内统一刊号:ISSN:11-2111/TF
  • 邮发代号:82-167
  • 获奖情况:
  • 中文核心期刊,冶金工业类核心期刊,中国科技论文统计源期刊
  • 国内外数据库收录:
  • 俄罗斯文摘杂志,美国化学文摘(网络版),荷兰文摘与引文数据库,美国工程索引,美国剑桥科学文摘,日本日本科学技术振兴机构数据库,中国中国科技核心期刊,中国北大核心期刊(2004版),中国北大核心期刊(2008版),中国北大核心期刊(2011版),中国北大核心期刊(2014版),中国北大核心期刊(2000版)
  • 被引量:13688