中文摘要：

本文采用球磨微波法合成锂离子电池正极材料Li3V2（P04）3／C，并研究了微波辐射时间对样品电化学性能的影响．结果表明，640W微波辐射18min合成的材料，结晶度高，粒径小面均匀．该电极5C倍率下首次放电比容量达101．3mAh·g^-1，300周期循环，其放电比容量仍保持100．8mAh·g^-1，展示出良好的应用前景．

英文摘要：

The cathode materials of LigV2 （PO4） 3/C were successfully synthesized by ball-milling assisted microwave method and the microwave irradiation time was also optimized. It is found that the Li3V2 （PO4 ）3/ C material obtained at a microwave power of 640 W for 18 rain shows the best electrochemical performance with the initial reversible capacity of 101.3 mAh·g^-1 and the remained 100.8mAh·g^-1 at 5C rate after 300 cycles. This excellent electrochemical capability may be resulted from good crystallinity, smaller and uniform particle size of the material, showing a great promise for battery applications.